自然科学版
陕西师范大学学报(自然科学版)
食品工程与营养科学
苹果渣中果胶的超声波辅助提取及特性研究
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田玉霞,仇农学,邓红,郭玉蓉
(陕西师范大学 食品工程与营养科学学院, 陕西 西安 710062)
田玉霞,女,硕士研究生,研究方向为食品质量过程控制.
摘要:
对超声波辅助提取苹果渣中的果胶进行研究,分析了超声频率、超声时间、料液比、提取温度和提取液pH值对果胶得率的影响,根据L16(45)设计正交试验,获得果胶最适提取条件为:超声频率28 kHz、超声时间50 min、料液比1∶20(g∶mL)、提取温度60℃、提取液pH=2.0.与传统酸法提取相比,最适提取时间由1.5 h缩短到50 min,得率由11.45%提高到13.64%.对所制备果胶的品质进行测定,结果表明:超声波对果胶的提取起到强化作用,而且不改变果胶的性质.气相色谱表明苹果果胶由果糖、鼠李糖、阿拉伯糖、木糖、甘露糖、葡萄糖、岩藻糖和半乳糖组成.
关键词:
超声波; 果胶; 苹果渣; 气相色谱
收稿日期:
2008-10-05
中图分类号:
Q539+.8
文献标识码:
A
文章编号:
1672-4291(2009)05-0100-05
基金项目:
农业部“苹果产业技术体系”(NYCYTX-08); 陕西师范大学优秀预研项目(2008)
Doi:
Study on Extraction of Pectin from Apple Pomace with Ultrasonic
TIAN Yu-xia, QIU Nong-xue*, DENG Hong, GUO Yu-rong
(College of Food Engineering and Nutritional Science, Shaanxi Normal University, Xi′an 710062, Shaanxi, China)
Abstract:
The extraction of pectin from apple pomace with ultrasonic was studied in this paper. The ultrasonic frequency, ultrasonic time, materials and solution ratio, extraction temperature and the pH of solution were analyzed. The experiment was arranged with L16(45). The optimal conditions of extraction were that ultrasonic frequency was 28 kHz, ultrasonic time was 50 min, proportion of materials and water was 1∶20 (g∶mL), extraction temperature was 60℃, and pH was 2.0. Compared with traditional method, the optimal time reduced from 1.5 h to 50 min, the extraction yield increased from 11.45% to 13.64%. At the same time, the quality of pectin was measured. The results showed that ultrasonic could strengthen the extraction of pectin from apple pomace, which didn't change the structure of pectin. The apple pectin polysaccharide was composed of fructose, rhamnose, arabinose, xylose, fucose, mannose, galactose and glucose.
KeyWords:
ultrasonic; pectin; apple pomace; gas chromatography