自然科学版
陕西师范大学学报(自然科学版)
化学与材料科学
磁性纳米复合粒子表面接枝聚苯乙烯磺酸钠的制备
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李艳利,杨红*,董旭刚
(应用表面与胶体化学教育部重点实验室; 陕西师范大学 化学与材料科学学院, 陕西 西安 710062)
李艳利,女,硕士研究生,主要从事高分子材料合成及性质研究.
摘要:
合成了聚苯乙烯磺酸钠接枝Fe3O4/SiO2纳米复合材料.通过表面引发原子转移自由基聚合在Fe3O4/SiO2磁性纳米粒子表面包覆了阴离子聚电解质(聚苯乙烯磺酸钠).利用透射电子显微镜(TEM),傅立叶变换红外光谱仪(FT-IR),震荡磁力计(VSM),X射线能谱仪(EDS),全自动X射线衍射仪(XRD)等仪器对所制备的复合材料进行了表征,成功制备了尺寸均一的聚苯乙烯磺酸钠接枝Fe3O4/SiO2核壳结构的纳米复合材料.
关键词:
Fe3O4/SiO2纳米粒子; 聚苯乙烯磺酸钠; 原子转移自由基聚合; 磁性聚合物复合材料
收稿日期:
2007-09-30
中图分类号:
TB383
文献标识码:
A
文章编号:
1672-4291(2008)03-0065-05
基金项目:
陕西省科技攻关项目(2004K07-G14)
Doi:
Preparation of poly (SStNa)-grafted magnetic nanocomposites
LI Yan-li, YANG Hong*, DONG Xu-gang
(Key Laboratory of Applied Surface and Colloid Chemistry, Ministry of Education; College of Chemistry and Materials Science, Shaanxi Normal University, Xi′an, 710062, Shaanxi China)
Abstract:
The paper describes the synthesis of the PSStNa-grafted magnetite/silica nanocomposites. The modified silica-coated Fe3O4 microspheres were prepared by grafting the anionic polyelectrolyte (PSStNa) using surface-initiated atom transfer radical polymerization (SI-ATRP). These hybrid microspheres are characterized by using various experimental techniques such as Transmission electron microscopy (TEM), X-ray diffraction (XRD), Energy dispersive X-ray spectrometry (EDS), Fourier transform infrared spectroscopy (FT-IR), and Vibration sample magnetometer (VSM). Based on this method, the uniform-sized Fe3O4/SiO2 magnetic composites covered with PSStNa could be obtained.
KeyWords:
Fe3O4/SiO2 nanoparticles; PSStNa; ATRP; Magnetic polymer composite materials