自然科学版
陕西师范大学学报(自然科学版)
物理学
磁控溅射参数对钛酸锶钡薄膜生长及介电性能的影响
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杨佳, 张运英, 谢晓康, 边小兵, 周剑平*
(陕西师范大学 物理学与信息技术学院, 陕西 西安 710119)
周剑平,男,教授,博士生导师。E-mail:zhoujp@snnu.edu.cn
摘要:
使用射频磁控溅射系统在Pt/SiO2/Si基片上沉积了Ba0.6Sr0.4TiO3 (BST)薄膜,研究了溅射过程中氧氩比与溅射总气压对BST薄膜生长过程及介电性能的影响。通过XRD衍射仪、原子力显微镜等对在不同条件下制备出的薄膜样品进行了性能测试和分析。结果表明:增加氧氩比能够增加薄膜表面晶粒尺寸,提升薄膜的结晶度,增加薄膜的介电常数并降低介电损耗,但同时也会降低薄膜的沉积速率;增加溅射气压会导致薄膜表面晶粒尺寸减小、结晶度降低,薄膜的沉积速率随着溅射气压的增加呈现先增加后降低(溅射气压大于2 Pa时)的趋势。
关键词:
射频磁控溅射; 钛酸锶钡薄膜; 表面形貌; 沉积速率; 介电性能
收稿日期:
2016-04-06
中图分类号:
O484
文献标识码:
A
文章编号:
1672-4291(2016)06-0026-05doi:10.15983/j.cnki.jsnu.2016.06.261
基金项目:
国家自然科学基金(51372148);中央高校基本科研业务费创新团队项目(GK201401003)
Doi:
Influence of magnetron sputtering parameters on the growth of barium strontium titanate thin films and dielectric properties
YANG Jia, ZHANG Yunying, XIE Xiaokang, BIAN Xiaobing, ZHOU Jianping*
(School of Physics and Information Technology, Shaanxi Normal University, Xi′an 710119, Shaanxi, China)
Abstract:
The Ba0.6Sr0.4TiO3 (BST) thin films were deposited on Pt/SiO2/Si substrates by an radio frequency magnetron sputtering.The influence of the ratio of O2 and Ar and pressure on the growth process and dielectric properties of BST thin films are investigated.The process of sputtering atmosphere on the BST film growth is studied with an atomic force microscope (AFM) and an X-ray diffractometer. The dielectric properties of BST films are measured by an Agilent impedance analyzer.The results show that the grain size, crystallinity and dielectric constant of thin films increase with the ratio of O2 and Ar, which decreases the dielectric loss but diminishes the depositing speed at the same time. The increasing of sputtering pressure lead the decrease of the grain size and crystallinity of BST thin films. The growth rate of BST thin films increases first and then decreases with sputtering pressure.
KeyWords:
radio frequency magnetron sputtering; BST thin films; surface morphology; growth rate; dielectric properties