自然科学版
陕西师范大学学报(自然科学版)
物理学
磁控溅射参数对钛酸锶钡薄膜生长及介电性能的影响
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谢晓康 缑园渊, 杨佳, 边小兵, 周剑平*
(陕西师范大学 物理学与信息技术学院, 陕西 西安 710119)
谢晓康,男,硕士研究生,研究方向为铁电薄膜的制备.Email:1029930629@qq.com.
摘要:
在Pt/Ti/SiO2/Si(110)衬底上利用射频磁控溅射法制备了Ba1-xSrxTiO3(BST)薄膜.基于薄膜的形核理论,研究了成膜时间、衬底温度、溅射功率、溅射气压、氧氩比、退火热处理等参数对薄膜的表面形貌和介电性能的影响.结果表明:在其他溅射参数一定的条件下,薄膜的厚度随溅射时间成指数关系增长;在退火温度600 ℃下热处理20 min薄膜完全晶化;调节衬底温度、溅射功率、溅射气压等参数有助于制备出表面致密、晶粒大小均匀、具有高介电常数和低损耗的BST薄膜.
关键词:
射频磁控溅射; 钛酸锶钡薄膜; 表面形貌; 介电性能
收稿日期:
2014-04-15
中图分类号:
O469
文献标识码:
文章编号:
1672-4291(2014)05003706
基金项目:
国家自然科学基金资助项目(51372148); 中央高校基本科研业务费创新团队资助项目(GK201401003).
Doi:
Effect of RFmagnetron sputtering parameters on the growth and dielectric property of BST thin film
XIE Xiaokang, GOU Yuanyuan, YANG Jia, BIAN Xiaobing, ZHOU Jianping*
College of Physics and Information Technology,Shaanxi Normal University, Xi′an 710119, Shaanxi, China)
Abstract:
BST thin films were prepared on Pt/Ti/SiO2/Si substrate by RFmagnetron sputtering. Based on the theory of film nucleation,the surface morphology and dielectric property of film influenced by RF sputtering parameters,such as the sputtering time,substrate temperature,sputtering power,sputtering pressure,ratio of oxygen and argon and annealing heat treatment were investigated.The results show that when others sputtering parameters controls, the film thickness increase in a exponential manner with sputtering time. The BST thin films were crystallized when annealing heat treatment in 20 minutes at 600 ℃. The BST thin films with compact surface, uniform crystalline grain sizes and high dielectric constant, low dielectric loss were obtained by adjusting the sputtering parameters.
KeyWords:
RFmagnetron sputtering; BST thin film; Surface morphology; dielectric property