自然科学版
陕西师范大学学报(自然科学版)
物理学
固相烧结法和反应烧结法制备G-La2Si2O7陶瓷的微波介电性能
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周晓娟, 刘鹏*, 韩赵翔, 程蕾
(陕西师范大学 物理学与信息技术学院, 陕西 西安 710062)
周晓娟,女,硕士研究生.研究方向为微波介电陶瓷.E-mail:yishengjum01@163.com.
摘要:
采用反应烧结法和传统固相反应法制备G-La2Si2O7陶瓷样品,并探究两种不同制备方法对G-La2Si2O7陶瓷的烧结性能、微观形貌、微波介电性能的影响.结果表明:传统固相法制备的G-La2Si2O7陶瓷性能优于反应烧结法制备材料,反应烧结法制备G-La2Si2O7陶瓷样品最佳的烧结温度为1 430 ℃,相对密度为90%,微波介电性能为:εr = 12.50, Q×f=26 594 GHz,τf=-23.99×10-6/℃.传统固相反应方法制备的G-La2Si2O7陶瓷样品最佳的烧结温度为1 415 ℃,相对密度为96.52%,微波介电性能为:εr =13.327,Q×f=33 900 GHz,τf =-34.9 ×10-6/℃.
关键词:
微波介电性能; 反应烧结; 固相反应; G-La2Si2O7陶瓷
收稿日期:
2013-03-14
中图分类号:
O469
文献标识码:
A
文章编号:
1672-4291(2013)05-0034-04
基金项目:
国家自然科学基金资助项目(51072110 ).
Doi:
Comparing microwave dielectric properties of G-La2Si2O7 ceramics prepared by reactive sintering process and conventional solid state reaction
ZHOU Xiao-juan, LIU Peng*, HAN Zhao-xiang, CHENG Lei
(College of Physics and Information Technology, Shaanxi Normal University, Xi′an 710062, Shaanxi, China)
Abstract:
La2Si2O7 ceramics prepared by reactive sintering process(RS) and conventional solid state reaction(SS) were investigated in the study. The influences of different processes on phase structures, surface morphologies, relative density and microwave dielectric properties were compared. The microwave dielectric properties of G-La2Si2O7 ceramics(SS) are better than G-La2Si2O7 ceramics(RS). The best sintered temperature, relative density and microwave dielectric properties of RS group G-La2Si2O7 ceramics are 1 430 ℃, 90%, εr = 12.50, Q×f=26 594 GHz and (τf = -23.99×10-6/℃, respectively. The best sintered temperature, relative density and microwave dielectric properties of SS group G-La2Si2O7 ceramics are 1 415 ℃, 96.52%,εr = 13.327,Q×f =33 900 GHz and τf =-34.9×10-6/℃, respectively.
KeyWords:
microwave dielectric property; reactive sintering; solid state reaction; G-La2Si2O7 ceramics